8.1.1 The (H)FID shall be adjusted as specified by the
instrument manufacturer. A propane in air span gas shall be used to optimize the
response on the most common operating range.
8.1.2 With the fuel and air flow rates set at
the manufacturer’s recommendations, a 350 ± 75 ppmC span
gas shall be introduced to the analyser. The response at a given fuel
flow shall be determined from the difference between the span gas
response and the zero gas response. The fuel flow shall be incrementally
adjusted above and below the manufacturer’s specification. The
span and zero response at these fuel flows shall be recorded. The
difference between the span and zero response shall be plotted and
the fuel flow adjusted to the rich side of the curve. This is the
initial flow rate setting which may need further optimization depending
on the results of the hydrocarbon response factors and the oxygen
interference check according to 8.2 and 8.3.
8.1.3 If the oxygen interference or the hydrocarbon
response factors do not meet the following specifications, the air
flow shall be incrementally adjusted above and below the manufacturer’s
specifications, 8.2 and 8.3 for each flow.
8.1.4 The optimization may optionally be conducted
using alternative procedures subject to the approval of the Administration.