4.0 Methods of Test [7]
Clasification Society 2024 - Version 9.40
Statutory Documents - IMO Publications and Documents - Circulars - Maritime Safety Committee - MSC/Circular.668 – Alternative Arrangements For Halon Fire-extinguishing Systems In Machinery Spaces And Pump-rooms – (Adopted on 22 December 1994)Amended by MSC/Circular.728 - Annex - Guidelines for the Approval of Equivalent Water-Based Fire-extinguishing Systems as Referred to in SOLAS 74 for Machinery Spaces and Cargo Pump-rooms - Appendix A - Component Manufacturing Standards of Equivalent Water-based Fire-extinguishing Systems - 4.0 Methods of Test [7]

4.0 Methods of Test [7]

4.1 General

 The following tests should be conducted for each type of nozzle. Before testing, precise drawings of parts and the assembly should be submitted together with the appropriate specifications (using SI units). Tests should be carried out at an ambient temperature of (20,±5)°C, unless other temperatures are indicated.

4.2 Visual examination [7.2]

 Before testing, nozzles should be examined visually with respect to the following points:

  • (a) marking

  • (b) conformity of the nozzles with the manufacturer's drawings and specification

  • (c) obvious defects

4.3 Body strength [7.3]

  4.3.1 The design load should be measured on ten automatic nozzles by securely installing each nozzle at room temperature, in a tensile/compression test machine and applying a force equivalent to the application of the rated working pressure.

 An indicator capable of reading deflection to an accuracy of 0.01 mm should be used to measure any change in length of the nozzle between its load bearing points. Movement of the nozzle shank thread in the threaded bushing of the test machine should be avoided or taken into account.

 The hydraulic pressure and load is then released and the heat responsive element is then removed by a suitable method. When the nozzle is at room temperature, a second measurement is to be made using the indicator.

 An increasing mechanical load to the nozzle is then applied at a rate not exceeding 500 N/minute, until the indicator reading at the load bearing point initially measured returns to the initial value achieved under hydrostatic load. The mechanical load necessary to achieve this should be recorded as the service load. Calculate the average service load.

  4.3.2 The applied load is then progressively increased at a rate not exceeding 500 N/minute on each of the five specimens until twice the average service load has been applied. Maintain this load for 15 ± 5 s.

 The load is then removed and any permanent elongation as defined in 3.6 is recorded.

4.4 Leak resistance and hydrostatic strength tests (see 3.8 ) [7.4]

  4.4.1 Twenty nozzles should be subjected to a water pressure of twice their rated working pressure, but not less than 34.5 bar. The pressure is increased from 0 bar to the test pressure, maintained at twice rated working pressure for a period of 3 min and then decreased to 0 bar. After the pressure has returned to 0 bar, it is increased to the minimum operating pressure specified by the manufacturer in not more than 5 s. This pressure is to be maintained for 15 s and then increased to rated working pressure and maintained for 15 s.

  4.4.2 Following the test of 4.4.1, the twenty nozzles should be subjected to an internal hydrostatic pressure of four times the rated working pressure. The pressure is increased from 0 bar to four times the rated working pressure and held there for a period of 1 minute. The nozzle under test should not rupture, operate or release any of its operating parts during the pressure increase nor while being maintained at four times the rated working pressure for 1 minute.

4.5 Functional test (see 3.5 ) [7.5]

  4.5.1 Nozzles having nominal release temperatures less than 78°C, should be heated to activation in an oven. While being heated, they should be subjected to each of the water pressures specified in 4.5.3 applied to their inlet. The temperature of the oven should be increased to 400 ± 20°C in 3 min measured in close proximity to the nozzle. Nozzles having nominal release temperatures exceeding 78°C should be heated using a suitable heat source. Heating should continue until the nozzle has activated.

  4.5.2 Eight nozzles should be tested in each normal mounting position and at pressures equivalent to the minimum operating pressure, the rated working pressure and the the average operating pressure. The flowing pressure should be at least 75% of the initial operating pressure.

  4.5.3 If lodgement occurs in the release mechanism at any operating pressure and mounting position, 24 more nozzles should be tested in that mounting position and at that pressure. The total number of nozzles for which lodgement occurs should not exceed 1 in the 32 tested at that pressure and mounting position.

  4.5.4 Lodgement is considered to have occurred when one or more of the released parts lodge in the discharge assembly in such a way a to cause the water distribution to be altered after the period of time specified in 3.5.1.

  4.5.5 In order to check the strength of the deflector/orifice assembly, three nozzles should be submitted to the functional test in each normal mounting position at 125 percent of the rated working pressure. The water should be allowed to flow at 125 percent of the rated working pressure for a period of 15 min.

4.6 Heat responsive element operating characteristics

4.6.1 Operating temperature test (see 3.3 ) [7.6]

 Ten nozzles should be heated from room temperature to 20 to 22°C below their nominal release temperature. The rate of increase of temperature should not exceed 20°C/min and the temperature should be maintained for 10 min. The temeprature should then be increased at a rate between 0.4°C/min to 0.7°C/min until the nozzle operates.

 The nominal operating temperature should be ascertained with equipment having an accuracy of ±0.35% of the nominal temperature rating or ±0.25°C, whichever is greater.

 The test should be conducted in a water bath for nozzles or separate glass bulbs having nominal release temperatures less than or equal to 80°C. A suitable oil should be used for higher-rated release elements. The liquid bath should be constructed in such a way that the temperature deviation within the test zone does not exceed 0.5%, or 0.5°C, whichever is greater.

4.6.2 Dynamic heating test (see 3.4 )

4.6.2.1 Plunge test

 Tests should be conducted to determine the standard and worst case orientations as defined in 1.4 and 1.5. Ten additional plunge test should be performed at both of the identified orientations. The worst case orientation should be as defined in 3.14.1. The RTI is calculated as described in 4.6.2.3 and 4.6.2.4 for each orientation, respectively. The plunge tests are to be conducted using a brass nozzle mount designed such that the mount or water temperature rise does not exceed 2°C for the duration of an individual plunge test up to a response time of 55 s. (The temperature should be measured by a thermocouple heatsinked and embedded in the mount not more than 8 mm radially outward from the root diameter of the internal thread or by a thermocouple located in the water at the centre of the nozzle inlet.) If the response time is greater than 55 s, then the mount or water temperature in degrees Celsius should not increase more than 0.036 times the response time in seconds for the duration of an individual plunge test.

 The nozzle under test should have 1 to 1.5 wraps of PTFE sealant tape applied to the nozzle threads. It should be screwed into a mount to a torque of 15 ± 3 Nm. Each nozzle is to be mounted on a tunnel test section cover and maintained in a conditioning chamber to allow the nozzle and cover to reach ambient temperature for a period of not less than 30 min.

 At least 25 ml of water, conditioned to ambient temperature, should be introduced into the nozzle inlet prior to testing. A time accurate to ±0.01 s with suitable measuring devices to sense the time between when the nozzle is plunged into the tunnel and the time it operates should be utilized to obtain the response time.

 A tunnel should be utilized with air flow and temperature conditionsfootnote at the test section (nozzle location) selected from the appropriate range of conditions shown in table 2. To minimize radiation exchange between the sensing element and the boundaries confining the flow, the test section of the apparatus should be designed to limit radiation effects to within ±3% of calculated RTI valuesfootnote.

Table 2 Plunge Oven Test Conditions

  Air Temperature ranges 4 Velocity ranges 5
Normal Temperature, ºC Standard Response, ºC Special response, ºC Fast Response, ºC Standard Response, m/s Special response, m/s Fast Response Nozzle, m/s
57 to 77 191 to 203 129 to 141 129 to 141 2.4 to 2.6 2.4 to 2.6 1.65 to 1.85
79 to 107 282 to 300 191 to 203 191 to 203 2.4 to 2.6 2.4 to 2.6 1.65 to 1.85
121 to 149 382 to 432 282 to 300 282 to 300 2.4 to 2.6 2.4 to 2.6 1.65 to 1.85
163 to 191 382 to 432 382 to 432 382 to 432 3.4 to 3.6 2.4 to 2.6 1.65 to 1.85
4.The selected air temperature should be known and maintained constant within the test section throughout the test section throughout the test to an accuracy of +/- 1 ºC for the air temperature range of 129 to 141 ºC within the test section and within +/- 2 ºC for all other air temperatures.
5. The selected air velocity should be known and maintained constant throughout the test to an accuracy of +/-0.03 m/s fpr velocities of 1.65 to 1.85 and 2.4 to 2.6 m/s and +/-0.04 for velocities 3.4 to 3.6 m/s.

 The range of permissible tunnel operating conditions is shown in table 2. The selected operating condition should be maintained for the duration of the test with the tolerances as specified by footnotes 10 and 11 in table 2.

4.6.2.2 Determination of Conductivity Factor (C) [7.6.2.2]

 The conductivity factor (C) should be determined using the prolonged plunge test (see 4.6.2.2.1) or the prolonged exposure ramp test (see 4.6.2.2.2).

4.6.2.2.1 Prolonged Plunge Test [7.6.2.2.1]

 The prolonged plunge test is an iterative process to determine C and may require up to twenty nozzle samples. A new nozzle sample must be used for each test in this section even if the sample does not operate during the prolonged plunge test.

 The nozzle under test should have 1 to 1.5 wraps of PTFE sealant tape applied to the nozzle threads. It should be screwed into a mount to a torque of 15 + 3 Nm. Each nozzle is to be mounted on a tunnel test section cover and maintained in a conditioning chamber to allow the nozzle and cover to reach ambient temperature for a period of not less than 30 min. At least 25 ml of water, conditioned to ambient temperature, should be introduced into the nozzle inlet prior to testing.

 A timer accurate to ±0.01 s with suitable measuring devices to sense the time between when the nozzle is plunged into the tunnel and the time it operates should be utilized to obtain the response time.

 The mount temperature should be maintained at 20 ± 0.5°C for the duration of each test. The air velocity in the tunnel test section at the nozzle location should be maintained with ±2% of the selected velocity. Air temperature should be selected and maintained during the test as specified in table 3.

Table 3 Plunge Oven Test Conditions for Conductivity Determinations

Nominal nozzle temperature, ºC Oven temperature, ºC Maximum variation of air temperature during test, ºC
57 85 to 91 ± 1.0
58 to 77 124 to 130 ± 1.5
78 to 107 193 to 201 ± 3.0
121 to 149 287 to 295 ± 4.5
163 to 191 402 to 412 ± 6.0

 The range of permissible tunnel operating conditions is shown in table 3. The selected operating condition should be maintained for the duration of the test with the tolerances as specified in table 3.

 To determine C, the nozzle is immersed in the test stream at various air velocities for a maximum of 15 minfootnote. Velocities are chosen such that actuation is bracketed between two successive test velocities. That is, two velocities must be established such that at the lower velocity (u1) actuation does not occur in the 15 min test interval. At the next higher velocity (uh), actuation must occur within the 15 min time limit. If the nozzle does not operate at the highest velocity, select an air temperature from table 3 for the next temperature rating.

 Test velocity selection should insure that:

 The test value of C is the average of the values calculated at the two velocities using the following equation:

where:
Δ T g = Actual gas (air) temperature minus the mount temperature (Tm) in °C.
Δ T ea = Mean liquid bath operating temperature minus the mount temperature (Tm) in °C.
u = Actual air velocity in the test section in m/s.

 The nozzle C value is determined by repeating the bracketing procedure three times and calculating the numerical average of the three C values. This nozzle C value is used to calculate all standard orientation RTI values for determining compliance with 3.14.1.

4.6.2.2.2 Prolonged Exposure Ramp Test [7.6.2.2.2]

 The prolonged exposure ramp test for the determination of the parameter C should be carried out in the test section of a wind tunnel and with the requirements for the temperature in the nozzle mount as described for the dynamic heating test. A preconditioning of the nozzle is not necessary.

 Ten samples should be tested of each nozzle type, all nozzles positioned in standard orientation. The nozzle should be plunged into an air stream of a constant velocity of 1 m/s ± 10% and an air temperature at the nominal temperature of the nozzle at the beginning of the test.

 The air temperature should then be increased at a rate of 1 ± 0.25°C/min until the nozzle operates. The air temperature, velocity and mount temperature should be controlled from the initiation of the rate of rise and should be measured and recorded at nozzle operation. The C value is determined using the same equation as in 4.6.2.2.1 as the average of the ten test values.

4.6.2.3 RTI Value Calculation [7.6.2.3]

 The equation used to determine the RTI value is a follows:

where:
t r = response time of nozzles in seconds
u = Actual air velocity in the test section of the tunnel in m/s from table 2
ΔT ea = Mean liquid bath operating temperature of the nozzle minus the ambient temperature in °C
ΔT g = Actual air temperature in the test section minus the ambient temperature in °C
C = Conductivity factor as determined in 4.6.2.2

4.6.2.4 Determination of Worst Case Orientation RTI

 The equation used to determine the RTI for the worst case orientation is as follows:

where:
t r-wc = Response time of the nozzles in seconds for the worst case orientation

 All variables are known at this time per the equation in paragraph 4.6.2.3 except RTIwc (Response Time Index for the worst case orientation) which can be solved iteratively per the above equation.

 In the case of fast response nozzles, if a solution for the worse case orientation RTI is unattainable, plunge testing in the worst case orientation should be repeated using the plunge test conditions under Special Response shown in table 2.

4.7 Heat Exposure Test [7.7]

4.7.1 Glass Bulb Nozzles (see 3.9.1 )

 Glass bulb nozzles having nominal release temperatures less than or equal to 80°C should be heated in a water bath from a temperature of (20 ± 5)°C to (20 ± 2)°C below their nominal release temperature. The rate of increase of temperature should not exceed 20°C/min. High temperature oil, such as silicone oil should be used for higher temperature rated release elements.

 This temperature should then be increased at a rate of 1°C/min to the temperature at which the gas bubble dissolves, or to a temperature 5°C lower than the nominal operating temperature, whichever is lower. Remove the nozzle from the liquid bath and allow it to cool in air until the gas bubble has formed again. during the cooling period, the pointed end of the glass bulb (seal end) should be pointing downwards. This test should be performed four times on each of four nozzles.

4.7.2 All Uncoated Nozzles (see 3.9.2 ) [7.7.2]

 Twelve uncoated nozzles should be exposed for a period of 90 days to a high ambient temperature that is 11°C below the nominal rating or at the temperature shown in table 4, whichever is lower, but not less than 49°C. If the service load is dependent on the service pressure, nozzles should be tested under the rated working pressure. After exposure, four of the nozzles should be subjected to the tests specified in 4.4.1, four nozzles to the test of 4.5.1. two at the minimum operating pressure and two at the rated working pressure, and four nozzles to the requirements 3.3. If a nozzle fails the applicable requirements of a test, eight additional nozzles should be tested as described above and subjected to the test in which the failure was recorded. All eight nozzles should comply with the test requirements.

Table 4 Test Temperatures for Coated and Uncoated Nozzles

Values in degrees Celsius
Nominal release temperature Uncoated nozzle test temperature Coated nozzle test temperature
57–60 49 49
61–77 52 49
78–107 79 66
108–149 121 107
150 to 191 149 149
192–246 191 191
247–302 246 246
303–343 302 302

4.7.3 Coated Nozzles (see 3.9.3 ) [7.7.3]

 In addition to the exposure test of 4.7.2 in an uncoated version, twelve coated nozzles should be exposed to the test of 4.7.2 using the temperatures shown in table 4 for coated nozzles.

 The test should be conducted for 90 days. During this period, the sample should be removed from the oven at intervals of approximately 7 days and allowed to cool for 2 h to 4 h. During this cooling period, the sample should be examined. After exposure, four of the nozzles should be subjected to the tests specified in 4.4.1, four nozzles to the test of 4.5.1; two at the minimum operating pressure and two at the rated working pressure, and four nozzles to the requirements of 3.3.

4.8 Thermal Shock Test for Glass Bulb Nozzles (see 3.10 ) [7.8]

 Before starting the test, condition at least 24 nozzles at room temperature of 20 to 25°C for at least 30 min.

 The nozzles should be immersed in a bath of liquid, the temperature of which should be 10 ± 2°C below the nominal release temperature of the nozzles. After 5 min, the nozzles are to be remove from the bath and immersed immediately in another bath of liquid, with the bulb seal downwards, at a temperature of 10 ± 1°C. Then test the nozzles in accordance with 4.5.1.

4.9 Strength Test for Release Elements [7.9]

4.9.1 Glass Bulbs (see 3.7.1 ) [7.9.1]

 At least 15 sample bulbs in the lowest temperature rating of each bulb type should be positioned individually in a test fixture using the sprinkler seating parts. Each bulb should then be subjected to a uniformly increasing force at a rate not exceeding 250 N/s in the test machine until the bulb fails.

 Each test should be conducted with the bulb mounted in new seating parts. The mounting device may be reinforced externally to prevent its collapse, but in a manner which does not interfere with bulb failure.

 Record the failure load for each bulb. Calculate the lower tolerance limit (TL1) for bulb strength. Using the values of service load recorded in 4.3.1, calculate the upper tolerance limit (TL2) for the bulb design load. Verify compliance with 3.7.1.

4.9.2 Fusible Elements (see 3.7.2 )

4.10 Water Flow Test (see 3.4.1 ) [7.10]

 The nozzle and a pressure gauge should be mounted on a supply pipe. The water flow should be measured at pressures ranging from the minimum operating pressure to the rated working pressure at intervals of approximately 10% of the service pressure range on two sample nozzles. In one series of tests, the pressure should be increased from zero to each value and, in the next series, the pressure shall be decreased from the rated pressure to each value. The flow constant, K, should be averaged from each series of readings, i.e., increasing pressure and decreasing pressure. During the test, pressures should be corrected for differences in height between the gauge and the outlet orifice of the nozzle.

4.11 Water Distribution and Droplet Size Tests

4.11.1 Water Distribution (see 3.4.2 )

 The tests should be conducted in a test chamber of minimum dimensions 7 m x 7 m or 300% of the maximum design area being tested, whichever is greater. For standard automatic nozzles, install a single open nozzle and then four open nozzles of the same type arranged in a square, at maximum spacings specified by the manufacturer, on piping prepared for this purpose. For pilot type nozzles, install a single nozzle and then the maximum number of slave nozzles at their maximum spacings, specified in the Manufacturer Design and Installation Instructions.

 The distance between the ceiling and the distribution plate should be 50 mm for upright nozzles and 275 mm for pendent nozzles. For nozzles without distribution plates, the distances shall be measured from the ceiling to the highest nozzle outlet.

 Recessed, flush and concealed type nozzles should be mounted in a false ceiling of dimensions not less than 6 m x 6 m and arranged symmetrically in the test chamber. The nozzles should be fitted directly into the horizontal pipework by means of “T" or elbow fittings.

 The water discharge distribution in the protected area below a single nozzle and between the multiple nozzles should be collected and measured by means of square measuring containers nominally 300 mm on a side. The distance between the nozzles and the upper edge of the measuring containers should be the maximum specified by the manufacturer. The measuring containers should be positioned centrally, beneath the single nozzle and beneath the multiple nozzles.

 The nozzles should be discharged both at the minimum operating and rated working pressures specified by the manufacturer and the minimum and maximum installation heights specified by the manufacturer.

 The water should be collected for at least 10 min to assist in characterizing nozzle performance.

4.11.2 Water Droplet Size (see 3.4.3 )

 The mean water droplet diameters. velocities, droplet size distribution, number density and volume flux should be determined at both the minimum and maximum flow rates specified by the manufacturer. Once the data is gathered, the method of the “Standard Practice for Determining Data Criteria and Processing for Liquid Drop Size Analysis" (ASTM E799-92) will be used to determine the appropriate sample size, class size widths, characteristic drop sizes and measured dispersion of the drop size distribution. This data should be taken at various points within the spray distribution as described in 3.4.3.

4.12 Corrosion Test [7.12]

4.12.1 Stress Corrosion Test for Brass Nozzle Parts (see 3.11.1 )

 Five nozzles should be subjected to the following aqueous ammonia test. The inlet of each nozzle should be sealed with a nonreactive cap, e.g., plastic.

 The samples are degreased and exposed for 10 days to a moist ammonia-air mixture in a glass container of volume 0.02 ± 0.01 m3.

 An aqueous ammonia solution, having a density of 0.94 g/cm3, should be maintained in the bottom of the container, approximately 40 mm below the bottom of the samples. A volume of aqueous ammonia solution corresponding to 0.01 ml per cubic centimetre of the volume of the container will give approximately the following atmospheric concentrations: 35% ammonia, 5% water vapour, and 60% air. The inlet of each sample should be sealed with a nonreactive cap, e.g. plastic.

 The moist ammonia-air mixture should be maintained as closely as possible at atmospheric pressure, with the temperature maintained at 34 ± 2°C. Provision should be made for venting the chamber via a capillary tube to avoid the build-up of pressure. Specimens should be shielded from condensate drippage.

 After exposure, rinse and dry the nozzles, and conduct a detailed examination. If a crack, delamination or failure of any operating part is observed, the nozzle(s) should be subjected to a leak resistance test at the rated pressure for 1 min and to the functional test at the minimum flowing pressure (see 3.1.5).

 Nozzles showing cracking, delamination or failure of any non-operating part should not show evidence of separation of permanently attached parts when subjected to flowing water at the rated working pressure for 30 min.

4.12.2 Stress-Corrosion Cracking of Stainless Steel Nozzle Parts (see 3.11.1 )

  4.12.2.1 Five samples are to be degreased prior to being exposed to the magnesium chloride solution.

  4.12.2.2 Parts used in nozzles are to be place in a 500-millilitre flask that is fitted with a thermometer and a wet condenser approximately 760 mm long. the flask is to be filled approximately one-half full with 42% by weight magnesium chloride solution, placed on a thermostatically-controlled electrically heated mantel, and maintained at a boiling temperature of 150 ± 1°C. The parts are to be unassembled, that is, not contained in a nozzle assembly. The exposure is to last for 500 hours.

  4.12.2.3 After exposure period, the test samples are to be removed from the boiling magnesium chloride solution and rinsed in deionized water.

  4.12.2.4 The test samples are then to be examined using a microscope having a magnification of 25X for any cracking, delamination, or other degradation as a result of the test exposure. Test samples exhibiting degradation are to be tested as described in 4.12.5.5 or 4.12.5.6, as applicable. test samples not exhibiting degradation are considered acceptable without further test.

  4.12.2.5 Operating parts exhibiting degradation are to be further tested as follows. Five new sets of parts are to be assembled in nozzle frames made of materials that do not alter the corrosive effects of the magnesium chloride solution on the stainless steel parts. These test samples are to be degreased and subjected to the magnesium chloride solution exposure specified in paragraph 4.12.5.2. following the exposure, the test samples should withstand, without leakage, a hydrostatic test pressure equal to the rated working pressure for 1 minute and then be subjected to the functional test at the minimum operating pressure in accordance with 4.5.1.

  4.12.2.6 Non-operating parts exhibiting degradation are to be further tested as follows. Five new sets of parts are to be assembled in nozzle frames made of materials that do not alter the corrosive effects of the magnesium chloride solution on the stainless steel parts. These test samples are to be degreased and subjected to the magnesium chloride solution exposure specified in paragraph 4.12.5.1. Following the exposure, the test samples should withstand a flowing pressure equal to the rated working pressure for 30 minutes without separation of permanently attached parts.

4.12.3 Sulphur Dioxide Corrosion Test (see 3.11.2 and 3.14.2 )

 Ten nozzles should be subjected to the following sulphur dioxide corrosion test. The inlet of each sample should be sealed with a nonreactive cap, e.g. plastic.

 The test equipment should consist of a 5 litre vessel (instead of a 5 litre vessel, other volumes up to 15 litre may be used in which case the quantities of chemicals given below shall be increased in proportion) made of heat-resistant glass, with a corrosion-resistant lid of such a shape as to prevent condensate dripping on the nozzles. The vessel should be electrically heated through the base, and provided with a cooling coil around the side walls. A temperature sensor placed centrally 160 mm ± 20 mm above the bottom of the vessel should regulate the heating so that the temperature inside the glass vessel is 45°C ± 3°C. During the test, water should flow through the cooling coil at a sufficient rate to keep the temperature of the discharge water below 30°C. This combination of heating and cooling should encourage condensation on the surfaces of the nozzles. The sample nozzles should be shielded from condensate drippage.

 The nozzles to be tested should be suspended in their normal mounting position under the lid inside the vessel and subjected to a corrosive sulphur dioxide atmosphere for 8 days. The corrosive atmosphere should be obtained by introducing a solution made up by dissolving 20 g of sodium thiosulphate (Na2S2O3H2O) crystals in 500 ml of water.

 For at least six days of the 8-day exposure period, 20 ml of dilute sulphuric acid consisting of 156 ml of normal H2SO4 (0.5 mol/liter) diluted with 844 ml of water should be added at a constant rate. After 8 days, the nozzles should be removed form the container and allowed to dry for 4 to 7 days at a temperature not exceeding 35°C with a relative humidity not greater than 70%.

 After the drying period. five nozzles should be subjected to a functional test at the minimum operating pressure in accordance with 4.5.1 and five nozzles should be subjected to the dynamic heating test in accordance with 3.14.2.

4.12.4 Salt Spray Corrosion Test (see 3.11.3 and 3.14.2 ) [7.12.3]

4.12.4.1 Nozzles Intended for Normal Atmospheres

 Ten nozzles should be exposed to a salt spray within a fog chamber. The inlet of each sample should be sealed with a nonreactive cap, e.g. plastic.

 During the corrosive exposure, the inlet thread orifice is to be sealed by a plastic cap after the nozzles have been filled with deionized water. The salt solution should be a 20% by mass sodium chloride solution in distilled water. The pH should be between 6.5 and 3.2 and the density between 1.126 g/ml and 1.157 g/ml when atomized at 35°C. Suitable means of controlling the atmosphere in the chamber should be provided. The specimens should be supported in their normal operating position and exposed to the salt spray (fog) in a chamber having a volume of at least 0.43 m3 in which the exposure zone shall be maintained at a temperature of 35 ± 2°C. The temperature should be recorded at least once per day, at least 7 hours apart (except weekends and holidays when the chamber normally would not be opened). Salt solution should be supplied from a recirculating reservoir through air-aspirating nozzles, at a pressure between 0.7 bar (0.07 MPa) and 1.7 bar (0.17 MPa). Salt solution runoff from exposed samples should be collected and should not return to the reservoir for recirculation. The sample nozzles should be shielded from condensate drippage.

 Fog should be collected from at least two points in the exposure zone to determine the rate of application and salt concentration. The fog should be such that for each 80 cm2 of collection area, 1 ml to 2 ml of solution should be collected per hour over a 16 hours period and the salt concentration shall be 20 ± 1% by mass.

 The nozzles should withstand exposure to the salt for a period of 10 days. After this period, the nozzles should be removed from the fog chamber and allowed to dry for 4 to 7 days at a temperature of 20 to 25°C in an atmosphere having a relative humidity not greater than 70%. Following the drying period, five nozzles should be submitted to the functional test at the minimum operating pressure in accordance with 4.5.1 and five nozzles should be subjected to the dynamic heating test in accordance with 3.14.2.

4.12.4.2 Nozzles Intended for Corrosive Atmospheres [7.12.3.2]

 Five nozzles should be subjected to the tests specified in 4.12.3.1 except that the duration of the salt spray exposure shall be extended from 10 days to 30 days.

4.12.5 Moist Air Exposure Test (see 3.11.4 and 3.14.2 ) [7.12.4]

 Ten nozzles should be exposed to a high temperature-humidity atmosphere consisting of a relative humidity of 98% ± 2% and a temperature of 95°C ± 4°C. The nozzles are to be installed on a pipe manifold containing deionized water. The entire manifold is to be placed in the high temperature humidity enclosure for 90 days. After this period, the nozzles should be removed from the temperature-humidity enclosure and allowed to dry for 4-7 days at a temperature of 25 ± 5°C in an atmosphere having a relative humidity of not greater than 70%. Following the drying period, five nozzles should be functionally tested at the minimum operating pressure in accordance with 4.5.1 and five nozzles should be subjected to the dynamic heating test in accordance with 3.14.2.

 At the manufacturer's option, additional samples may be furnished for this test to provide early evidence of failure. The additional samples may be removed from the test chamber at 30-day intervals for testing.

4.13 Nozzle Coating Tests [7.13]

4.13.1 Evaporation Test (see 3.12.1 ) [7.13.1]

 A 50 cm3 sample of wax or bitumen should be placed in a metal or glass cylindrical container, having a flat bottom, an internal diameter of 55 mm and an internal height of 35 mm. The container, without lid, should be placed in an automatically controlled electric, constant ambient temperature oven with air circulation. The temperature in the oven should be controlled at 16°C below the nominal release temperature of the nozzle, but at not less than 50°C. The sample should be weighed before and after 90 days exposure to determine any loss of volatile matter; the sample should meet the requirements of 3.12.1.

4.13.2 Low-Temperature Test (see 3.12.2 ) [7.13.2]

 Five nozzles, coated by normal production methods, whether with wax, bitumen or a metallic coating, should be subjected to a temperature of -10°C for a period of 24 hours. On removal from the low-temperature cabinet, the nozzles should be exposed to normal ambient temperature for a least 30 min before examination of the coating to the requirements of 3.12.2.

4.14 Heat-Resistance Test (see 3.15 ) [7.14]

 One nozzle body should be heated in an oven at 800°C for a period of 15 min, with the nozzle in its normal installed position. The nozzle body should then be removed, holding it by the threaded inlet, and should be promptly immersed in a water bath at a temperature of approximately 15°C. It should meet the requirements of 3.15.

4.15 Water-Hammer Test (see 3.13 ) [7.15]

 Five nozzles should be connected, in their normal operating position, to the test equipment. After purging the air from the nozzles and the test equipment, 3,000 cycles of pressure varying from 4 ± 2 bar ((0.4 ± 0.2)MPa) to twice the rated working pressure should be generated. The pressure should be raised from 4 bar to twice the rated working pressure at a rate of 60 ± 10 bar/s. At least 30 cycles of pressure per minute should be generated. The pressure should be measured with an electrical pressure transducer.

 Visually examine each nozzle for leakage during the test. After the test, each nozzle should meet the leakage resistance requirement of 3.8.1 and the functional requirements of 3.5.1 at the minimum operating pressure.

4.16 Vibration Test (see 3.16 ) [7.16]

  4.16.1 Five nozzles should be fixed vertically to a vibration table. They should be subjected at room temperature to sinusoidal vibrations. The direction of vibration should be along the axis of the connecting thread.

  4.16.2 The nozzles should be vibrated continuously from 5 Hz to 40 Hz at a maximum rate of 5 min/octave and an amplitude of 1 mm (1/2 peak-to-peak value). If one or more resonant points are detected, the nozzles after coming to 40 Hz, should be vibrated at each of these resonant frequencies for 120 hours/number of resonances. If no resonances are detected, the vibration from 5 Hz to 40 Hz should be continued for 120 hours.

  4.16.3 The nozzle should then be subjected to the leakage test in accordance with 3.8.1 and the functional test in accordance with 3.5.1 at the minimum operating pressure.

4.17 Impact Test (see 3.17 ) [7.17]

 Five nozzles should be tested by dropping a mass onto the nozzle along the axial centreline of waterway. The kinetic energy of the dropped mass at the point of impact should be equivalent to a mass equal to that of the test nozzle dropped from a height 1 m. See Figure 2. The mass is to be prevented from impacting more than once upon each sample.

Figure 2 Impact Test Apparatus

 Following the test a visual examination of each nozzle shall show no signs of fracture, deformation, or other deficiency. If none is detected, the nozzles should be subjected top the leak resistance test, described in 4.4.1. Following the leakage test, each sample should meet the functional test requirement of 4.5.1 at a pressure equal to the minimum flowing pressure.

4.18 Lateral Discharge Test (see 3.18 ) [7.19]

 Water is to be discharged from a spray nozzle at the minimum operating and rated working pressure. A second automatic nozzle located at the minimum distance specified by the manufacturer is mounted on a pipe parallel to the pipe discharging water.

 The nozzle orifices or distribution plates (if used), are to be placed 550 mm, 356 mm and 152 mm below a flat smooth ceiling for three separate tests, respectively at each test pressure. The top of a square pan measuring 305 mm square and 102 mm deep is to be positioned 152 mm below the heat responsive element for each test. The pan is filled with 0.47 litres of heptane. After ignition the automatic nozzle is to operate before the heptane is consumed.

4.19 30 Day Leakage Test (see 3.19 ) [7.20]

 Five nozzles are to be installed on a water filled test line maintained under a constant pressure of twice the rated working pressure for 30 days at an ambient temperature of (20 ± 5°C).

 The nozzles should be inspected visually at least weekly for leakage. Following completion of this 30 day test, all samples should meet the leak resistance requirements specified in 3.2.4 and should exhibit no evidence of distortion or other mechanical damage.

4.20 Vacuum Test (see 3.20 ) [7.21]

 Three nozzles should be subjected to a vacuum of 460 mm of mercury applied to a nozzle inlet for 1 min at an ambient temperature of (20 ± 5°C). Following this test, each sample should be examined to verify that no distortion or mechanical damage has occurred and then should meet the leak resistance requirements specified in 4.4.1.

4.21 Clogging Test (see 3.22 ) [7.28]

  4.21.1 The water flow rate of an open water mist nozzle with its strainer or filter should be measured at its rated working pressure. The nozzle and strainer or filter should then be installed in test apparatus described in Figure 3 and subjected to 30 minutes of continuous flow at rated working pressure using contaminated water which has been prepared in accordance with 4.21.3.

Figure 3 Clogging test apparatus

  4.21.2 Immediately following the 30 minutes of continuous flow with contaminated water, the flow rate of the nozzle and strainer or filter should be measured at rated working pressure. No removal, cleaning or flushing of the nozzle, filter or strainer is permitted during the test.

  4.21.3 The water used during the 30 minutes of continuous flow at rated working pressure specified in 4.21.1 should consist of 60 litres of tap water into which has been mixed 1.58 kilograms of contaminants which sieve as described in table 6. The solution should be continuously agitated during the test.

Table 6 Contaminant for the Contaminated Water Cycling Test

SIEVE DESIGNATION * NOMINAL SIEVE OPENING, MM GRAMS OF CONTAMINANT (± 5 PERCENT)
PIPE SCALE TOP SOIL SAND
No. 25 0.706 456 200
No. 50 0.297 82 82 327
No. 100 0.150 84 6 89
No. 200 0.074 81 21
No. 325 0.043 153 3
  TOTAL 400 544 640

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